From 920b4c37596e3327af41e11fcaa726525aef3355 Mon Sep 17 00:00:00 2001 From: Nicole Jung Date: Sun, 22 Oct 2023 23:02:51 +0200 Subject: [PATCH] Update reactions_test.mdx --- docs/repo/details_standards/reactions_test.mdx | 16 +++++++++------- 1 file changed, 9 insertions(+), 7 deletions(-) diff --git a/docs/repo/details_standards/reactions_test.mdx b/docs/repo/details_standards/reactions_test.mdx index 5da5f89d..4fb89929 100644 --- a/docs/repo/details_standards/reactions_test.mdx +++ b/docs/repo/details_standards/reactions_test.mdx @@ -49,18 +49,20 @@ Valid options are: #### Giving the amount of chemicals used as reagent or reactant - Reactant quantities should be reported in weight, volume (if applicable), molar units and equivalents. Valid options are: -(a) quinoline-4-carboxylic acid (20.0 g, 115 mmol, 1.00 equiv), +(a) quinoline-4-carboxylic acid (20.0 g, 115 mmol, 1.00 equiv),
(b) …20.0 g of quinoline-4-carboxylic acid (115 mmol, 1.00 equiv) #### Giving the amount of chemicals as a product of a reaction -The yield of a product of a reaction is given for pure products. If the product is gained as crude compound (due to whatever reason) this has to be clearly given in the form: "crude product was gained". The yield of a reaction should be given in weight, mmol/mol and percentage in parentheses after the compound name (or its equivalent). The informqtion in parentheses is separated by a comma. -Valid options are: -(a) Methyl quinoline-4-carboxylate (16.4 g, 87.5 mmol, 76% yield) was isolated as a colorless solid. -(b) Methyl quinoline-4-carboxylate (16.4 g, 87.5 mmol) was isolated as a colorless solid in 76% yield. -(c) Methyl quinoline-4-carboxylate was isolated as a colorless solid in 76% yield (16.4 g, 87.5 mmol). +The yield of a product of a reaction is given for pure products. The yield of a reaction should be given in weight, mmol/mol and percentage in parentheses after the compound name (or its equivalent). The informqtion in parentheses is separated by a comma. +Valid options are:
+(a) Methyl quinoline-4-carboxylate (16.4 g, 87.5 mmol, 76% yield) was isolated as a colorless solid.
+(b) Methyl quinoline-4-carboxylate (16.4 g, 87.5 mmol) was isolated as a colorless solid in 76% yield.
+(c) Methyl quinoline-4-carboxylate was isolated as a colorless solid in 76% yield (16.4 g, 87.5 mmol).
+If the product is gained as crude compound which was not purified this has to be clearly given in the form: "crude product was gained". If the compound was obtained with impurities, the impurities have to be mentioned in the analyses of the characterization of the sample, and the impurities have to be included to the yield of the reaction by changing the purity/concentration value of the sample. In such a case, please mention the correction of yield in the deacription as follows (example a)):
+(a) Methyl quinoline-4-carboxylate (16.4 g, 90% purity, 78.8 mmol, 68% yield) was isolated as a colorless solid.
:::caution Change in sample required -Information on the purity of a product need to be added in the sample entity of the repository +Information on the purity of a product need to be added in the sample entity of the repository. A purity of 90% corresponds to a the value of 0.9 in the field concentration of a sample. :::